Low temperature plasma and ozone are widely used in air disinfection and purification, medical disinfection, food processing, water treatment, environmental resource protection, fruit and vegetable preservation, sterilization and deworming of agricultural greenhouse crops, granary mold and insect proof, etc. The use of ozone sterilization and poisoning has the characteristics of good effect, fast action, no secondary pollution after use, and no residue. Therefore, the equipment for ozone disinfection archives has been used by part of archives and libraries. At the same time, ozone, as a powerful oxidant, has long been suspected of possibility of paper archives damage when sterilized, causing fading of writing and printing inks, as well as damage to human body due to poor ozone leakage. In order to answer these questions, sufficient experimental verification must be carried out on the plasma ozone archives disinfection cabin. This paper records the whole experiment process in detail.